Auinger, M.; Vogel, D.; Vogel, A.; Spiegel, M.; Rohwerder, M.: A novel laboratory set-up for investigating surface and interface reactions during short term annealing cycles at high temperatures. Review of Scientific Instruments 84, 085108 (2013)
Swaminathan, S.; Rohwerder, M.; Rohwerder, M.; Spiegel, M.: Temperature and dew point dependent segregation of phosphorus and sulfur in Fe–Mn–P–S model alloy. Surface and Coatings Technology 205 (16), pp. 4089 - 4093 (2011)
Asteman, H.; Spiegel, M.: A comparison of the oxidation behaviours of Al2O3 formers and Cr2O3 formers at 700 °C - Oxide solid solutions acting as a template for nucleation. Corrosion Science 50 (6), pp. 1734 - 1743 (2008)
Swaminathan, S.; Spiegel, M.: Effect of alloy composition on the selective oxidation of ternary Fe–Si–Cr, Fe–Mn–Cr model alloys. Surface and Interface Analysis 40 (3-4), pp. 268 - 272 (2008)
Mardare, C. C.; Spiegel, M.; Savan, A.; Ludwig, A.: Investigation of thin coatings from Mn–Co system deposited by PVD on metallic interconnects for SOFC Applications. Material Science Forum 595-598, pp. 797 - 804 (2008)
Swaminathan, S.; Koll, T.; Pohl, M.; Wieck, A. D.; Spiegel, M.: Hot-dip galvanizing simulation of model alloys and industrial steel grades: Correlation between surface chemistry and wettability. Steel Res. Int. 79 (1), pp. 66 - 72 (2008)
Asteman, H.; Spiegel, M.: Investigation of the HCl (g) attack on pre-oxidized pure Fe, Cr, Ni and commercial 304 steel at 400 °C. Corrosion Science 49 (9), pp. 3626 - 3637 (2007)
Li, Y. S.; Niu, Y.; Spiegel, M.: High temperature interaction of Al/Si-modified Fe–Cr alloys with KCl. Corrosion Science 49 (4), pp. 1799 - 1815 (2007)
Ruh, A.; Spiegel, M.: Thermodynamic and kinetic consideration on the corrosion of Fe, Ni and Cr beneath a molten KCl-ZnCl2 micture. Corr.Sci. 48, pp. 679 - 695 (2006)
Ruh, A.; Spiegel, M.: Influence of gas phase composition on the kinetics of chloride melt induced corrosion of pure iron. Mater. and Corr. 57, pp. 237 - 243 (2006)
Sánchez Pastén, M.; Spiegel, M.: High temperature corrosion of metallic materials in simulated waste incineration environments at 300-600 °C. Mater. and Corr. 57, pp. 192 - 195 (2006)
Li, Y. S.; Spiegel, M.; Shimada, S.: Corrosion behaviour of model alloys with NaCl–KCl coating. Materials Chemistry and Physics 93 (1), p. 217 - 217 (2005)
Hydrogen in aluminium can cause embrittlement and critical failure. However, the behaviour of hydrogen in aluminium was not yet understood. Scientists at the Max-Planck-Institut für Eisenforschung were able to locate hydrogen inside aluminium’s microstructure and designed strategies to trap the hydrogen atoms inside the microstructure. This can…
We plan to investigate the rate-dependent tensile properties of 2D materials such as metal thin films and PbMoO4 (PMO) films by using a combination of a novel plan-view FIB based sample lift out method and a MEMS based in situ tensile testing platform inside a TEM.
This project aims to investigate the influence of grain boundaries on mechanical behavior at ultra-high strain rates and low temperatures. For this micropillar compressions on copper bi-crystals containing different grain boundaries will be performed.
Oxidation and corrosion of noble metals is a fundamental problem of crucial importance in the advancement of the long-term renewable energy concept strategy. In our group we use state-of-the-art electrochemical scanning flow cell (SFC) coupled with inductively coupled plasma mass spectrometer (ICP-MS) setup to address the problem.
For understanding the underlying hydrogen embrittlement mechanism in transformation-induced plasticity steels, the process of damage evolution in a model austenite/martensite dual-phase microstructure following hydrogenation was investigated through multi-scale electron channelling contrast imaging and in situ optical microscopy.
We will investigate the electrothermomechanical response of individual metallic nanowires as a function of microstructural interfaces from the growth processes. This will be accomplished using in situ SEM 4-point probe-based electrical resistivity measurements and 2-point probe-based impedance measurements, as a function of mechanical strain and…
Hydrogen induced embrittlement of metals is one of the long standing unresolved problems in Materials Science. A hierarchical multiscale approach is used to investigate the underlying atomistic mechanisms.
Hydrogen embrittlement affects high-strength ferrite/martensite dual-phase (DP) steels. The associated micromechanisms which lead to failure have not been fully clarified yet. Here we present a quantitative micromechanical analysis of the microstructural damage phenomena in a model DP steel in the presence of hydrogen.