Auinger, M.; Vogel, D.; Vogel, A.; Spiegel, M.; Rohwerder, M.: A novel laboratory set-up for investigating surface and interface reactions during short term annealing cycles at high temperatures. Review of Scientific Instruments 84, 085108 (2013)
Swaminathan, S.; Rohwerder, M.; Rohwerder, M.; Spiegel, M.: Temperature and dew point dependent segregation of phosphorus and sulfur in Fe–Mn–P–S model alloy. Surface and Coatings Technology 205 (16), pp. 4089 - 4093 (2011)
Asteman, H.; Spiegel, M.: A comparison of the oxidation behaviours of Al2O3 formers and Cr2O3 formers at 700 °C - Oxide solid solutions acting as a template for nucleation. Corrosion Science 50 (6), pp. 1734 - 1743 (2008)
Swaminathan, S.; Spiegel, M.: Effect of alloy composition on the selective oxidation of ternary Fe–Si–Cr, Fe–Mn–Cr model alloys. Surface and Interface Analysis 40 (3-4), pp. 268 - 272 (2008)
Mardare, C. C.; Spiegel, M.; Savan, A.; Ludwig, A.: Investigation of thin coatings from Mn–Co system deposited by PVD on metallic interconnects for SOFC Applications. Material Science Forum 595-598, pp. 797 - 804 (2008)
Swaminathan, S.; Koll, T.; Pohl, M.; Wieck, A. D.; Spiegel, M.: Hot-dip galvanizing simulation of model alloys and industrial steel grades: Correlation between surface chemistry and wettability. Steel Res. Int. 79 (1), pp. 66 - 72 (2008)
Asteman, H.; Spiegel, M.: Investigation of the HCl (g) attack on pre-oxidized pure Fe, Cr, Ni and commercial 304 steel at 400 °C. Corrosion Science 49 (9), pp. 3626 - 3637 (2007)
Li, Y. S.; Niu, Y.; Spiegel, M.: High temperature interaction of Al/Si-modified Fe–Cr alloys with KCl. Corrosion Science 49 (4), pp. 1799 - 1815 (2007)
Ruh, A.; Spiegel, M.: Thermodynamic and kinetic consideration on the corrosion of Fe, Ni and Cr beneath a molten KCl-ZnCl2 micture. Corr.Sci. 48, pp. 679 - 695 (2006)
Ruh, A.; Spiegel, M.: Influence of gas phase composition on the kinetics of chloride melt induced corrosion of pure iron. Mater. and Corr. 57, pp. 237 - 243 (2006)
Sánchez Pastén, M.; Spiegel, M.: High temperature corrosion of metallic materials in simulated waste incineration environments at 300-600 °C. Mater. and Corr. 57, pp. 192 - 195 (2006)
Li, Y. S.; Spiegel, M.; Shimada, S.: Corrosion behaviour of model alloys with NaCl–KCl coating. Materials Chemistry and Physics 93 (1), p. 217 - 217 (2005)
Hydrogen in aluminium can cause embrittlement and critical failure. However, the behaviour of hydrogen in aluminium was not yet understood. Scientists at the Max-Planck-Institut für Eisenforschung were able to locate hydrogen inside aluminium’s microstructure and designed strategies to trap the hydrogen atoms inside the microstructure. This can…
In this project we investigate the hydrogen distribution and desorption behavior in an electrochemically hydrogen-charged binary Ni-Nb model alloy. The aim is to study the role of the delta phase in hydrogen embrittlement of the Ni-base alloy 718.
We plan to investigate the rate-dependent tensile properties of 2D materials such as HCP metal thin films and PbMoO4 (PMO) films by using a combination of a novel plan-view FIB based sample lift out method and a MEMS based in situ tensile testing platform inside a TEM.
Oxidation and corrosion of noble metals is a fundamental problem of crucial importance in the advancement of the long-term renewable energy concept strategy. In our group we use state-of-the-art electrochemical scanning flow cell (SFC) coupled with inductively coupled plasma mass spectrometer (ICP-MS) setup to address the problem.
For understanding the underlying hydrogen embrittlement mechanism in transformation-induced plasticity steels, the process of damage evolution in a model austenite/martensite dual-phase microstructure following hydrogenation was investigated through multi-scale electron channelling contrast imaging and in situ optical microscopy.
We will investigate the electrothermomechanical response of individual metallic nanowires as a function of microstructural interfaces from the growth processes. This will be accomplished using in situ SEM 4-point probe-based electrical resistivity measurements and 2-point probe-based impedance measurements, as a function of mechanical strain and…
Hydrogen induced embrittlement of metals is one of the long standing unresolved problems in Materials Science. A hierarchical multiscale approach is used to investigate the underlying atomistic mechanisms.
Hydrogen embrittlement affects high-strength ferrite/martensite dual-phase (DP) steels. The associated micromechanisms which lead to failure have not been fully clarified yet. Here we present a quantitative micromechanical analysis of the microstructural damage phenomena in a model DP steel in the presence of hydrogen.