Scientific Events

Host: Prof. Gerhard Dehm

Aberration-corrected STEM and ultra-high energy resolution EELS

Aberration-corrected STEM and ultra-high energy resolution EELS
Electron microscopy has advanced very significantly in the last two decades. Electron-optical correction of aberrations, which we introduced for the scanning transmission electron microscope (STEM) in 1997, has allowed STEMs to reach sub-Å resolution from 2002 on. It has led to new STEM capabilities, such as atomic-resolution elemental mapping, and determining the type of single atoms by electron energy loss spectroscopy (EELS) and energy-dispersive X-ray spectroscopy (EDXS). More recently, we have focused on Ultra-High Energy Resolution EELS (UHERE). We have developed a monochromator and a spectrometer that use multipolar optics similar to the optics of aberration correctors, plus several stabilization methods, and we have reached <5 meV energy resolution at 30 keV primary energy. This has opened up a new field: vibrational spectroscopy in the electron microscope. When collecting large-angle scattering events, vibrational spectroscopy can lead to sub-nm spatial resolution, and when collecting small-angle scattering angle events, it can produce EEL spectra with the electron beam positioned tens of nm away from the probed area. The second geometry has led to a powerful new technique: aloof vibrational analysis of materials, which avoids significant radiation damage. Even more recently, we have focused on combining the analytical techniques with in-situ sample treatment. Our progress includes cooling the sample to liquid N2 temperature in a side-entry holder capable of reaching better than 1 Å resolution. My talk will review these developments, and illustrate them by application examples. [more]

Atomistic modeling of grain boundary segregation in transition metals

Atomistic modeling of grain boundary segregation in transition metals

Synthesis and characterization of tungsten-based composites for high-temperature applications

Synthesis and characterization of tungsten-based composites for high-temperature applications

Spatially Resolved Texture and Microstructure Evolution of Additively Manufactured and Gas Gun Deformed 304L Stainless Steel; Investigated by Neutron Diffraction and Electron Backscatter Diffraction

Spatially Resolved Texture and Microstructure Evolution of Additively Manufactured and Gas Gun Deformed 304L Stainless Steel; Investigated by Neutron Diffraction and Electron Backscatter Diffraction

Size Effects in Metals: On the Role of Internal Boundaries across the Scales

MPIE Colloquium
Size effects are a key ingredient to control and improve the mechanical behaviour of metallic microstructures and miniaturized components. The analysis of size effects in metals has received continuous attention in the past two decades, both experimentally and numerically. This lecture focuses on the role of grain and phase boundaries in restricting dislocation motion, giving rise to size effects. Some essential features of a thermodynamically consistent model for a grain boundary are presented, which accounts for the grain boundary energy and defect structure and evolution. The role of a phase boundary is investigated with a dislocation transport driven crystal plasticity model, revealing the explicit role of the plastic phase contrast and phase boundary resistance. Interesting size effects are thereby recovered. Size effects can also be eliminated or inhibited by other microstructural mechanisms. Two cases are addressed to illustrate this. The first case reveals the role of dislocation climb and its effectiveness in dissolving dislocation pile-ups. The second case concerns a very thin austenitic film in martensite, whereby the particular structure of the phase and its interface give rise to preferential sliding mechanisms that circumvent the common dislocation driven size effects.This lecture addresses the strengthening role of internal boundaries, constituting a major con- tribution to size effects in metals. It is shown that besides dislocation pile-ups, other mechanisms may be essential. For grain boundaries, the defect absorption and redistribution matters. For phase boundaries, phase contrast in dislocation transport alone already contributes to size effects. Moreover, dislocation-pile ups can be dissolved through climb at higher temperatures or circum- vented by other particular micromechanisms. This analysis effectively illustrates that predicting size effects in metals quantitatively remains a major challenge. References [1] van Beers P.R.M., Kouznetsova V.G., Geers M.G.D.: Defect redistribution within a continuum grain boundary plasticity model. J. Mech. Phys. Solids 83:243-262, 2015.[2] Dogge M.M.W., Peerlings R.H.J., Geers M.G.D.: Interface modeling in continuum dislocation transport. Me- chanics of Materials. 88:30-43, 2015.[3] Geers M.G.D., Cottura M., Appolaire B., Busso E.P., Forest S.,Villani A.: Coupled glide-climb diffusion- enhanced crystal plasticity. J. Mech. Phys. Solids. 70:136-153, 2014.[4] Maresca F., Kouznetsova V.G., Geers M.G.D.: Subgrain lath martensite mechanics: a numerical-experimental analysis. J. Mech. Phys. Solids. 73:69-83, 2014.[5] Maresca F., Kouznetsova V.G., Geers M.G.D.: Deformation behaviour of lath martensite in multi-phase steels. Scripta Materialia 110:74-77, 2016.[6] Maresca F., Kouznetsova V.G., Geers M.G.D.: Predictive modeling of interfacial damage in substructured steels: application to martensitic microstructures. Mod. Sim. Mat. Sc. Engng. 24(2):025006, 2016.[7] Du C., Hoefnagels J.P.M, Vaes R., Geers M.G.D.: Block and sub-block boundary strengthening in lath marten- site, Scripta Materialia,116:117-121, 2016.[8] Du C., Hoefnagels J.P.M, Vaes R., Geers M.G.D.: Plasticity of lath martensite by sliding of substructure boundaries, Scripta Materialia 120:37-40, 2016. [more]

Phase Transformations under Rapid Heating in Metallic Micro- and Nanolaminates

Phase Transformations under Rapid Heating in Metallic Micro- and Nanolaminates

Publishing in Material Science - and how to Maximize your success

Publishing your research results is an integral – if not the most important – part of your research. In this talk, some insight in the publishing process at the inhouse editorial offices of the successful journal family of Advanced Materials will be given. I will clarify the workflow at a publishing house from the moment the manuscript arrives until it is published and emphasize the role of the editor in that process. In the second part, I concentrate specifically on the requirements for successful publication in our high-impact journals and explain our requirements for acceptable manuscripts in our journals – and which pit falls authors should avoid in the preparation and submission process. [more]
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